I allowed my students to choose between two separation type laboratories. About two thirds of the class chose to separate the flavoring out of a grape of cherry soda. The rest of the students used paper chromatography to determine if red-40 dye was in a specific type of candy.
At Chem Ed 2015, a teacher from Texas showed me this quick and dirty way to do a distillation that the kids can do. I forgot her name. "Lady from Texas", let me just say "thank you". If you are reading this, please shoot me an email and I will be more than happy to give you credit. It worked really well.